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題名: Synthesis of the Chiral Triphosphine (S,S)-PhP(CH2CHMeCH2PPh2)2 and Its Metal Complexes
作者: Jia, Guochen;Lee, Hon Man;Ian D. Williams
貢獻者: 化學系
日期: 1996-10
上傳時間: 2014-08-14T04:28:22Z
出版者: American Chemical Society
摘要: The chiral triphosphine ligand (S,S)-PhP(CH2CHMeCH2PPh2)2, ttp*, was synthesized by the reaction of (S)-Ph2PCH2CHMeCH2Cl and PhPH2 in the presence of LDA. Reactions of ttp* with RuCl2(PPh3)3, [RhCl(COD)]2, and CoCl2 produced RuCl2(ttp*), RhCl(ttp*), and CoCl2(ttp*), respectively. These compounds were characterized by elemental analysis and multinuclear NMR spectroscopy. The structure of RhCl(ttp*) has been determined by X-ray diffraction.
關聯: Organometallics, 15(20): 4235-4239
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